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Diaqua­Bis­[4-(Dimethyl­Amino)­Benzoato-Κo]Bis­(Nicotinamide-Κn1)Zinc(Ii) Dihydrate

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Hökelek et al. - 2010 - Diaqua­bis­[4-(dimethyl­amino)­benzoato-κO]bis­(ni.pdf (442.4Kb)
Date
2010
Author
Sağlam, Ertuğrul Gazi
Tercan, Barış
Aybirdi, Özgür
Necefoğlu, Hacali
Hökelek, Tuncer
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Abstract
In the centrosymmetric title structure, [Zn(C9H10NO2)2(C6H6N2O)2(H2O)2]·2H2O, the ZnII cation, located on an inversion center, is coordinated by two 4-(methyl­amino)­benzoate anions, two nicotinamide ligands and two water mol­ecules in a slightly distorted octa­hedral geometry. The dihedral angle between the carboxyl­ate group and the attached benzene ring is 3.09 (9)°, while the pyridine and benzene rings are oriented at a dihedral angle of 77.10 (4)°. The uncoordinated water mol­ecule is linked to nicotinamide ligands by O—H⋯O hydrogen bonds. In the crystal, inter­molecular N—H⋯O, O—H⋯O and C—H⋯O hydrogen bonds link the mol­ecules into a three-dimensional network. A weak N—H⋯π inter­action also occurs.
URI
https://doi.org/10.1107/S1600536810046854
https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3011468/
http://hdl.handle.net/11655/18309
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